| 杯[4]芳烃巯基吡啶衍生物的合成 |
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| 引用本文： | 孔晓伟,蒋忠良,李乾坤. 杯[4]芳烃巯基吡啶衍生物的合成[J]. 精细与专用化学品, 2011, 19(10): 16-18 |
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| 作者姓名： | 孔晓伟 蒋忠良 李乾坤 |
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| 作者单位： | 1. 同济大学化学系,上海,200092
2. 辽宁工程招标公司,辽宁沈阳,110005 |
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| 摘 要： | 以对叔丁基苯酚为起始原料,通过缩合得到对叔丁基杯[4]芳烃,再对其下沿酚羟基进行化学修饰,得到具有化学活性的杯[4]衍生物,该化合物与具有活泼氢的4巯基吡啶反应制得新的含N、S杯芳烃衍生物,总收率15.3%。
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| 关 键 词： | 杯[4]芳烃 衍生物 合成 |
The synthesis of p-tert-butylcalix[4]arene derivative of pyridinethiol |
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| KONG Xiao-wei,JIANG Zhong-liang,LI Qian-kun. The synthesis of p-tert-butylcalix[4]arene derivative of pyridinethiol[J]. Fine and Specialty Chemicals, 2011, 19(10): 16-18 |
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| Authors: | KONG Xiao-wei JIANG Zhong-liang LI Qian-kun |
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| Affiliation: | KONG Xiao-wei~1,JIANG Zhong-liang~1,LI Qian-kun~2 (1.Department of Chemistry,Tongji University,Shanghai 200092,China,2.Liaoning Engineering Bidding Company,Shenyangl 10005,China) |
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| Abstract: | p-tert-Butlycalix[4]arene was synthesized via condensation of p-tert-phenol with formaldehyde. After substitution and reduction reactions,a novel calix[4]arene derivative of N and S containing compound was obtained with an overall yield of 15.3%. |
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| Keywords: | calix[4]arene derivative synthesis |
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