| 溶剂热法制备锂离子电池SnS_2负极材料 |
| |
| 引用本文： | 周从雨,张颖,汪大云,韩恩山.溶剂热法制备锂离子电池SnS_2负极材料[J].河北工业大学学报,2010(4). |
| |
| 作者姓名： | 周从雨 张颖 汪大云 韩恩山 |
| |
| 作者单位： | 河北工业大学化工学院; |
| |
| 摘 要： | 采用结晶四氯化锡和硫代乙酰胺为原料,乙醇为溶剂,在不同反应物浓度下制备了SnS2粉体.用X射线衍射(XRD),扫描电镜(SEM),循环伏安(CV)和恒电流充放电对其进行研究.结果表明,当反应物浓度降为初始反应浓度的1/3时,制备出的样品为纳米片状六方相晶体结构,在0.01～1.2V间,以0.5C(C=646mA·g-1)的电流对其进行充放电,30次循环后容量仍保持在301mAhg1以上.具有良好的循环稳定性,说明纳米SnS2是一种有希望的锂离子电池负极材料.
|
| 关 键 词： | SnS2 负极材料 溶剂热法 锂离子电池 电化学性能 |
Preparation of SnS_2 for Anode Materials of Lithium Ion Batteries by Solvothermal Technology |
| |
| ZHOU Cong-yu,ZHANG Ying,WANG Da-yun,HAN En-shan.Preparation of SnS_2 for Anode Materials of Lithium Ion Batteries by Solvothermal Technology[J].Journal of Hebei University of Technology,2010(4). |
| |
| Authors: | ZHOU Cong-yu ZHANG Ying WANG Da-yun HAN En-shan |
| |
| Abstract: | SnS2 powders were prepared by solvothermal technology in the solvent of absolute ethanol using stannic chloride hydrated and thioacetamide at different concentrations.The powders were studied by X-ray diffraction(XRD),scanning electron microscopy(SEM),cyclic voltammetry(CV) and constant current charge/discharge measurements.The results showed that the prepared sample with the shape of nano-flake and hexagonal crystal structure,when the reactants concentrations decreased to the 1/3 of the initial,could retai... |
| |
| Keywords: | SnS2 anode materials solvothermal technology lithium ion batteries electrochemical properties |
| 本文献已被 CNKI 万方数据 等数据库收录！ |
|
