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混合合金法添加DyH_x对烧结Nd-Fe-B磁体性能和微观结构的影响
引用本文:刘国军,李家节,赵睿,张文臣,李卫.混合合金法添加DyH_x对烧结Nd-Fe-B磁体性能和微观结构的影响[J].功能材料,2010,41(1).
作者姓名:刘国军  李家节  赵睿  张文臣  李卫
作者单位:钢铁研究总院,功能材料研究所,北京,100081
基金项目:国家高技术研究发展计划(863计划)资助项目(2007AA03Z116,2007AA03Z438);;国家自然科学基金资助项目(50871032,50571035)
摘    要:以Nd31.5FebalB6.0Co1.2Cu0.04(质量分数,%)为母合金,添加不同含量DyHx粉研究Dy对Nd-Fe-B磁体性能和微观结构的影响。研究发现,Dy未扩散到主相晶粒中,主要分布在晶界相中;Dy使磁体晶粒得到细化、均匀化,异常长大晶粒基本消失,晶粒边界结构得到改善;添加0.5%(质量分数)的DyHx粉可以明显提高磁体矫顽力Hcj,但添加量超过1.0%(质量分数),磁体矫顽力Hcj增幅变小,磁体密度严重下降。

关 键 词:晶粒尺寸  矫顽力  晶界相  形核场  

Effect of blending DyH_x addition on the properties and microstructures of sintered Nd-Fe-B magnet
LIU Guo-jun,LI Jia-jie,ZHAO Rui,ZHANG Wen-chen,LI Wei.Effect of blending DyH_x addition on the properties and microstructures of sintered Nd-Fe-B magnet[J].Journal of Functional Materials,2010,41(1).
Authors:LIU Guo-jun  LI Jia-jie  ZHAO Rui  ZHANG Wen-chen  LI Wei
Affiliation:Division of Functional Materials;Central Iron & Steel Research Institute;Beijing 100081;China
Abstract:The effect of Dy on the properties and microstructures of sintered Nd-Fe-B with addition of various amounts of DyHx powder to Nd31.5FebalB6.0Co1.2Cu0.04(wt%),as a precursor alloy,has been investigated. It is found that Dy is only located in the intergranular phases,and there is no diffusion of Dy into the matrix phases;It makes the grain more refined and uniform,and can effectively restrain the abnormal grain growth. Meanwhile,the microstructure of grain boundary has been improved;In addition,intrinsic coer...
Keywords:grain size  coercivity  intergranular phase  nucleation field  
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