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Microstructure,mechanical properties and toughening mechanisms of graphene reinforced Al2O3-WC-TiC composite ceramic tool material
Authors:Xuchao Wang  Jun Zhao  Enzhao Cui  Shiping Song  Hao Liu  Weitian Song
Affiliation:1. Key Laboratory of High Efficiency and Clean Mechanical Manufacture of MOE, School of Mechanical Engineering, Shandong University, Jinan, 250061, China;2. National Demonstration Center for Experimental Mechanical Engineering Education (Shandong University), Jinan, 250061, China
Abstract:The low fracture toughness of Al2O3-based ceramics limited their practical application in cutting tools. In this work, graphene was chosen to reinforce Al2O3-WC-TiC composite ceramic tool materials by hot pressing. Microstructure, mechanical properties and toughening mechanisms of the composite ceramic tool materials were investigated. The results indicated that the more refined and denser composite microstructures were obtained with the introduction of graphene. The optimal flexural strength, Vickers hardness, indentation fracture toughness were 646.31?±?20.78?MPa, 24.64?±?0.42?GPa, 9.42?±?0.40?MPa?m1/2, respectively, at 0.5?vol% of graphene content, which were significantly improved compared to ceramic tool material without graphene. The main toughening mechanisms originated from weak interfaces induced by graphene, and rugged fractured surface, grain refinement, graphene pull-out, crack deflection, crack bridging, micro-crack and surface peeling were responsible for the increase of fracture toughness values.
Keywords:Graphene  Composite ceramic tool material  Microstructure  Mechanical properties  Toughening mechanisms
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