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Preparation of low-shrinkage and high-performance alumina ceramics via incorporation of pre-sintered alumina powder based on Isobam gelcasting
Authors:Lin Lv  Yuju Lu  Xiaoyan Zhang  Yugu Chen  Wenlong Huo  Wei Liu  Jinlong Yang
Affiliation:1. School of Materials Science and Engineering, North University of China, Taiyuan, 030051, China;2. State Key Lab of New Ceramics and Fine Processing, School of Materials Science and Engineering, Tsinghua University, Beijing, 100084, China
Abstract:Mechanically robust alumina ceramics with low shrinkage were successfully prepared via gelcasting using Isobam as the gelling agent and pre-sintered alumina powder as the raw material for the first time. The influence of amount of pre-sintered alumina powder and powder's pre-sintering temperature on the viscosity of suspension and mechanical properties of low-shrinkage alumina ceramics were systematically investigated. The results showed that low-shrinkage alumina ceramics with flexural strength of 294.5?±?33.0?MPa, linear shrinkage of 7.79% and relative density of 91.5% can be obtained with the addition of 60?wt% alumina powder pre-sintered at 1600?°C. This convenient and facile approach is promising to fabricate low-shrinkage alumina ceramics with large sizes, high dimensional accuracy and complex shapes.
Keywords:Low shrinkage  Alumina ceramic  Isobam  Pre-sintered powder  Gelcasting
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