Synthesis of rod-shaped LaNi5 alloy via solid reduction method |
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Affiliation: | 1. A. Che?kowski Institute of Physics, University of Silesia in Katowice, Uniwersytecka 4, 40-007 Katowice, Poland;2. Silesian Center for Education and Interdisciplinary Research, University of Silesia in Katowice, 75 Pu?ku Piechoty 1A, 41-500 Chorzów, Poland;3. Institute of Materials Science, University of Silesia in Katowice, 75 Pu?ku Piechoty 1A, 41-500 Chorzów, Poland;4. l''Institut des Molécules et Matériaux du Mans UMR CNRS 6283, Université du Maine, Avenue Olivier Messiaen, 72085 Le Mans, France |
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Abstract: | A novel chemical synthesis technique that a large quantity of rod-shaped LaNi5 alloy has been successfully synthesized using a solid reduction method was reported. The as-prepared alloy, proven via the XRD spectrum, was single-phased and hexagonal. The SEM and TEM photographs showed that the alloy was rod-shaped with a diameter in the range of 300–500 nm, and length of about 6–10 μm. The SAED pattern of LaNi5 alloy clearly indicated the orientation alignment along the c-axis. |
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