Hydrothermal synthesis,crystal structure and characterization of LiCoP5O14·H2O: A new condensed layered penta phosphate crystals |
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| Affiliation: | 1. Poznan University of Technology, Poznan, Poland;2. Polish Geological Institute, Warsaw, Poland;1. Department of Chemistry, Osmania University, Hyderabad, 500007;2. University College of Science, Saifabad, Osmania University, Hyderabad, 500004 |
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| Abstract: | A new family of condensed hydrated lithium cobalt penta phosphate (LiCoP5O14·H2O) crystals were synthesized by hydrothermal technique and characterized by X-ray diffraction method. The compound crystallizes in monoclinic system with space group P21/c and cell parameters a = 10.788(4) Å, b = 9.761(3) Å, c = 9.788(5) Å, β = 101.249(1) Å, Z = 4, exhibiting layer type polymeric structure. DTA study indicates that this compound has low thermal stability and magnetically frequency dependent paramagnetic behaviour. |
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