Preparation,characterization and dielectric properties of Ba3−xSrxM4Ti4O21 (M = Nb,Ta and 0 ≤ x ≤ 3) ceramics |
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| Affiliation: | 1. Research & Development Center, Korea Testing Certification, Gunpo, Republic of Korea;2. Department of Industrial Engineering, Graduate School of Ajou University, Suwon, Republic of Korea;3. Reliability Physics Research Center, Korea Electronic Technology, Seongnam, Republic of Korea;1. School of Physics and Information Technology, Shaanxi Normal University, Xi’an 710062, China;2. School of Science, Xi’an University of Posts and Telecommunications, Xi’an 710121, China;1. School of Science, Xi''an University of Architecture and Technology, Xi''an 710055, China;2. Key Laboratory of Northwest Water Resource, Environment and Ecology, MOE, Xi''an University of Architecture and Technology, Xi''an 710055, China;1. Guangdong Provincial Key Laboratory of Nanophotonic Functional Materials and Devices, School of Information and Photoelectronic Science and Engineering, South China Normal University, Guangzhou 510006, China;2. Research Resources Center, South China Normal University, Guangzhou 510006, China |
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| Abstract: | Ba3−xSrxM4Ti4O21 (M = Nb, Ta and 0 ≤ x ≤ 3) ceramics have been prepared through solid state ceramic route. The structure and microstructure of the compositions have been studied using powder X-ray diffraction and Scanning Electron Microscopic studies. In the present study, both Ba3Nb4Ti4O21 and Ba3Ta4Ti4O21 are obtained as single phase compositions whereas strontium rich compositions exhibit multiphase in nature. Energy dispersive X-ray analysis has been performed to identify the nature of additional phases present in the strontium rich compositions. The dielectric constant, dielectric loss and temperature variation of dielectric constant of the well sintered ceramic specimens have been studied in the low frequency region (< 13 MHz) using an impedance analyzer. The present study reveals that high dielectric compositions can be realized by Sr-substitution in the BaO–TiO2–Nb2O5/Ta2O5 ternary systems. |
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