| 微波条件下两种煤丙酮萃取物的GC/MS分析 |
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| 引用本文： | 鞠彩霞,徐伟,宗志敏,魏贤勇. 微波条件下两种煤丙酮萃取物的GC/MS分析[J]. 煤炭转化, 2007, 30(1): 1-4 |
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| 作者姓名： | 鞠彩霞 徐伟 宗志敏 魏贤勇 |
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| 作者单位： | 枣庄学院化学化工系,277160,山东枣庄;中国矿业大学化学工程学院,221008,江苏徐州 |
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| 基金项目： | 国家自然科学基金 , 国家重点基础研究发展计划(973计划) , 高等学校博士学科点专项科研项目 |
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| 摘 要： | 以丙酮作为溶剂,在微波辐射条件下对兖州煤和神府煤进行萃取,并利用气相色谱/质谱联用(GC/MS)技术对萃取物进行分析.结果表明:萃取物主要由芳烃和脂肪烃组成.在兖州煤的萃取物中芳烃主要是茶系化合物,而在神府煤的萃取物中检测出的芳烃以菲系为主;在兖州煤的萃取物中检测出多种异构烷烃,而在神府煤中只检测出一种异构烷烃.
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| 关 键 词： | 煤 萃取 微波 GC/MS |
| 修稿时间： | 2006-09-15 |
GC/MS ANALYSIS BITUMINOUS OF ACETONE-EXTRACTION FROM COALS UNDER MICROWAVE TWO KINDS OF IRRADIATION |
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| Ju Caixia,Xu Wei,Zong Zhimin,Wei Xianyong. GC/MS ANALYSIS BITUMINOUS OF ACETONE-EXTRACTION FROM COALS UNDER MICROWAVE TWO KINDS OF IRRADIATION[J]. Coal Conversion, 2007, 30(1): 1-4 |
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| Authors: | Ju Caixia Xu Wei Zong Zhimin Wei Xianyong |
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| Affiliation: | 1.Department of Chemistry, Zaozhuang Normal College,277160 Zaozhuang Shandong 2. School of Chemical Engineering and Technology, China University of Mining and Technology, 221008 Xuzhou J iangsu |
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| Abstract: | Yanzhou and Shenfu coals are extracted using acetone as solvent under microwave irradiation and the extracts are analyzed with GC/MS. The results show that the extracts consist mainly of arenes and alkanes; arenes in the extracts from Yanzhou coal are detected to occur mainly in the form of naphthalene and alkylnaphthalenes, while the detected arenes in extracts from Shenfu coal are dominated . The extracts from Yanzhou coal are detected to occur as a number of branched alkanes, while the extracts from Shenfu coal are detected to occur as only one branched alkane. |
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| Keywords: | coal extraction microwave GC/MS |
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