| 高效液相色谱法测定饮料中安赛蜜、苯甲酸、山梨酸、糖精钠含量 |
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| 引用本文： | 巩强,张组维. 高效液相色谱法测定饮料中安赛蜜、苯甲酸、山梨酸、糖精钠含量[J]. 中国食品添加剂, 2006, 0(5): 152-153 |
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| 作者姓名： | 巩强 张组维 |
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| 作者单位： | 1. 山西省食品质量监督检验中心,030012
2. 山西农业大学动物科技学院,030801 |
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| 摘 要： | 采用液相色谱条件在波长230nm下，以0．02mol／L乙酸铵：甲醇（95：5）为流动相，快速测定饮料中苯甲酸、山梨酸、糖精钠、安赛蜜含量，样品处理简便快捷。方法添加标准回收率分别为99％、98％、97％、99％。本法与国家标准检验方法（GB／T5009．140—2003、GB／T5009．28—2003、GB／T5009-29—2003）比较，经配对t检验（P〉0．05）无显著性差异。
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| 关 键 词： | 高效液相色谱 苯甲酸 山梨酸 糖精钠 安赛蜜 |
| 文章编号： | 1006-2513(2006)05-0152-02 |
| 收稿时间： | 2006-06-30 |
| 修稿时间： | 2006-06-30 |
Detection of benzoic acid,sorbic acid,sodium saccharin,acesulfame patassium to beverage with high performance liquid chromatography |
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| GONG Qiang,ZHANG Zu-wei. Detection of benzoic acid,sorbic acid,sodium saccharin,acesulfame patassium to beverage with high performance liquid chromatography[J]. China Food Additives, 2006, 0(5): 152-153 |
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| Authors: | GONG Qiang ZHANG Zu-wei |
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| Affiliation: | 1. Shanxi Food Quality Supervision and Inspection Center 030012; College of Animal Science and Veterinary Medicine, Shanxi Agricultural University 030801 |
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| Abstract: | A high performance liquid chromatographic method was developed for determination of benzoic acid,sorbic acid,soluble saccharin,acesulfame patassium in beverage.Sample were rapidly determinated at wavelength 230nm with 0.02mol/ L ammonium acetate:methanol (95:5 V/V) as mobile phase with high performance liquid chromatography.Recoveries were 99%,98%,97%,99%,respectively.The experimental result is uniform GB/T5009.28-2003,GB/T5009.29-2003,GB/T5009.140-2003 by conjugate T test. |
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| Keywords: | high performance liquid chromatography benzoic acid sorbic acid sodium saccharin acesulfame patassium |
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