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Hydrothermal synthesis of hexagonal ZnO clusters
Authors:Yu Chen  Qian Shi  Feng Zheng
Affiliation:a School of Materials Science and Engineering, Central South University, Changsha, Hunan 410083, PR China
b Key Laboratory of Non-ferrous Materials, Ministry of Education, Central South University, Changsha, Hunan 410083, PR China
Abstract:Hydrothermal process was applied to synthesize zinc oxide nanocrystals. X-ray powder diffraction and scanning electron microscopy were used to analyze the crystal structure and surface morphology. XRD pattern analysis showed that the ZnO clusters are single hexagonal phase of wurtzite structure (space group P63 mc) with no impurity of Zn and Zn(OH)2. Also, SEM images revealed that the size of a single ZnO crystal is between 200-500 nm in diameter and 2-5 μm in length. The influence of potassium iodide (KI) as a surfactant on the crystallinity of ZnO has been investigated.
Keywords:Hydrothermal   Zinc oxide (ZnO) clusters   Wurtzite structure   Potassium iodide
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