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A simple route to synthesis of BaCO3 nanostructures in water/ethylene glycol mixed solvents
Authors:Ming-Guo Ma  Ying-Jie Zhu  Jie-Fang Zhu
Affiliation:a State Key Laboratory of High Performance Ceramics and Superfine Microstructure, Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 200050, PR China
b Graduate School of the Chinese Academy of Sciences, Beijing, PR China
c Beijing Institute of Petro-Chemical Technology, Beijing 102617, PR China
Abstract:Barium carbonate (BaCO3) nanostructures with different morphologies were synthesized using Ba(NO3)2 and (NH4)2CO3 in the water/ethylene glycol (EG) mixed solvents by oil bath heating at 80 °C for 30 min. The molar ratio of water to EG had an effect on the morphology of BaCO3. The products were characterized by X-ray powder diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and high-resolution transmission electron microscopy (HRTEM).
Keywords:BaCO3  Synthesis  Water  Ethylene glycol
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