Synthesis,characterization, thermal study,and crystal structure of a new layered alkaline earth metal sulfonate: Sr[C2H4(SO3)2] |
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| Authors: | Tolulope O Salami Stephanie N Patterson Victoria D Jones Antonio Masello Khalil A Abboud |
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| Affiliation: | 1. Department of Chemistry, Valdosta State University, Valdosta, GA 31698-0170, USA;2. Department of Chemistry, University of Florida, Gainesville, FL 32611-7200, USA |
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| Abstract: | A rare two-dimensional layered inorganic–organic hybrid material, strontium sulfonate SrC2H4(SO3)2] was synthesized by hydrothermal reaction of strontium chloride hexahydrate and ethane disulfonic acid at 160 °C. Single-crystal X-ray diffraction was utilized for structural determination. Data showed that the compound, crystallized in the monoclinic system and space group of C2/c. With cell parameters a = 8.3183(7) Å, b = 5.4416(5) Å and c = 14.9784(13) Å. The new material was extensively studied by DRIFT-infrared spectroscopy, thermogravimetric analysis, SEM and powder X-ray diffraction. Results show that the compound is thermally stable. |
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