| 高纯度烟碱的制备 |
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| 引用本文： | 储志兵,水恒福,陈建民. 高纯度烟碱的制备[J]. 应用化工, 2007, 36(1): 102-104 |
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| 作者姓名： | 储志兵 水恒福 陈建民 |
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| 作者单位： | 1. 安徽工业大学,化学与化工学院,安徽,马鞍山,243002
2. 复旦大学,环境科学与工程系,上海,200433 |
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| 摘 要： | 介绍了以废弃烟草为原料,经皂化、蒸馏、酸化、浓缩、碱化及有机溶剂萃取制备高纯度烟碱的新方法。确定了制备高纯度烟碱的最优工艺为:取1 000 g废弃烟草,加入3 L 0.1 mol/L的NaOH水溶液于60℃皂化4 h,蒸馏皂化液得到烟碱馏出液,酸化、浓缩、氯仿萃取,氯仿液用无水硫酸钠脱水后,减压浓缩得到高纯度烟碱,制得的烟碱纯度达到了99.23%,整个过程的收率为82.7%。
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| 关 键 词： | 废弃烟草 烟碱 提取 |
| 文章编号： | 1671-3206（2007）01-0102-03 |
| 修稿时间： | 2006-09-13 |
Preparation of high purity nicotine |
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| CHU Zhi-bing,SHUI Heng-fu,CHEN Jian-min. Preparation of high purity nicotine[J]. Applied chemical industry, 2007, 36(1): 102-104 |
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| Authors: | CHU Zhi-bing SHUI Heng-fu CHEN Jian-min |
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| Abstract: | New method for the production of nicotine from waste tobacco by saponification,distillation,(acidification),inspissation,extraction had been investigated.Thus,1 000 g waste tobacco was saponified by 3 L of 0.1 mol/L sodium hydroxide solution at 60 ℃ for 4 h.Nicotine solution was obtained from saponification solution by distillation,after acidification,inspissation and extraction with chloroform,nicotine was obtained from chloroform solution by distillation with purity of 99.23% and yield of 82.7%. |
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| Keywords: | waste tobacco nicotine extraction |
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