Hydrothermal Synthesis and Characterization of a Novel Organic Inorganic Hybrid Compound [Co(dien)_2](dienH_3)(H_3O)_7[P_2Mo_5O_(23)]_2·14H_2O |
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作者姓名: | 赵卫锋 |
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作者单位: | State Key |
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基金项目: | Funded by the Natural Science Foundation of Hubei Province (No. 2003ABA085),Key Laboratory for Silicate Materials Science and Engineering (Wuhan University of Technology), Ministry of Education (No.2003-SJSJJ-15) |
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摘 要: | A new compound,[Co(dien)2](dienH3)(H3O)7[P2Mo5O23]2·14H2O, has been hydrothermallly synthesized by using Na2MoO4,CoCl2, H3PO4 and dien, and structurally characterized by elemental analysis, X-ray powder diffraction analysis, SEM, IR and TG analysis. The results show that the compound is composed of a polyanion [P2Mo5O23]212- , complex [Co(dien)2]2 cation, protonated [dienH3]3 , and forteen crystallization water molecule.
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