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固相微萃取-气相色谱-质谱联用法检测小白牛肉的挥发性成分
引用本文:魏晋梅,罗玉柱,王继卿,师希雄,刘秀,胡江,成述儒,李少斌. 固相微萃取-气相色谱-质谱联用法检测小白牛肉的挥发性成分[J]. 食品工业科技, 2011, 0(9): 73-75
作者姓名:魏晋梅  罗玉柱  王继卿  师希雄  刘秀  胡江  成述儒  李少斌
作者单位:1. 甘肃农业大学研究测试中心,甘肃兰州730070/甘肃省草食动物生物技术重点实验室,甘肃兰州730073
2. 甘肃农业大学食品科学与工程学院,甘肃兰州,730070
3. 甘肃省草食动物生物技术重点实验室,甘肃兰州,730073
基金项目:国家科技支撑计划课题(2007BAD52B05,2009BAC53B06); 甘肃省重点实验室建设计划(085RTSA004)
摘    要:采用固相微萃取-气相色谱-质谱联用法(Solid Phase Microextraction-Gas Chromatography-Mass Spectrometry)分析检测了小白牛肉的挥发性风味物质,共分离检测得到125种化合物,定性和定量鉴定得到49种化合物,占总化合物的93.994%,其中醛类15种、醇类10种、烃类8种、酯类3种、酚类3种、酸类2种、杂环类2种、酮类6种。初步判断己醛、壬醛、辛醛、1-辛烯-3-醇、1-(2-硝基丙基)-环己醇、庚醛、二叔丁基对甲酚、N-己酸乙烯酯、2-戊基呋喃、1-辛醇等为小白牛肉的主体香味成分。

关 键 词:小白牛肉  挥发性成分  固相微萃取  气相色谱-质谱

Analysis of odors from veal by Solid Phase Microextraction-Gas Chromatography-Mass Spectrometry
WEI Jin-mei,,LUO Yu-zhu,,WANG Ji-qing,SHI Xi-xiong,LIU Xiu,HU Jiang,CHENG Shu-ru,LI Shao-bin. Analysis of odors from veal by Solid Phase Microextraction-Gas Chromatography-Mass Spectrometry[J]. Science and Technology of Food Industry, 2011, 0(9): 73-75
Authors:WEI Jin-mei    LUO Yu-zhu    WANG Ji-qing  SHI Xi-xiong  LIU Xiu  HU Jiang  CHENG Shu-ru  LI Shao-bin
Affiliation:WEI Jin-mei1,2,LUO Yu-zhu1,*,WANG Ji-qing1,SHI Xi-xiong3,LIU Xiu1,HU Jiang2,CHENG Shu-ru2,LI Shao-bin2(1. Instrumental Research and Analysis Center,Gansu Agricultural University,Lanzhou 730070,China,2. Gansu Key Laboratory of Herbivorous Animal Biotechnology,Lanzhou 730073,3. College of Food Science and Engineering,China)
Abstract:A method for the determination of volatile compounds from veal using Solid Phase Microextraction-Gas Chromatography-Mass Spectrometry(SPME-GC-MS)was presented.Totally 125 volatile flavor compounds were detected,and 49 components were identified by qualitative and quantitative analysis.The content of them account for 93.994%,and they were 15 aldehydes,10 alcohols,8 hydrocarbons,3 ester,3 phenols,2 acids,6 ketones and 2 heterocyclic compounds.Among these compounds,Hexanal,Nonanal,Octanal,1-Octen-3-ol,1-(2-nit...
Keywords:veal  volatile flavor constituents  SPME  GC-MS  
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