| 气相色谱/质谱法测定JP-10的成分及纯度 |
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| 引用本文： | 李艳玲,冀克俭,刘元俊,高迪,高岩立,赵晓刚.气相色谱/质谱法测定JP-10的成分及纯度[J].含能材料,2015,23(8):776-780. |
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| 作者姓名： | 李艳玲 冀克俭 刘元俊 高迪 高岩立 赵晓刚 |
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| 作者单位： | 中国兵器工业集团第五三研究所, 山东 济南 250031,中国兵器工业集团第五三研究所, 山东 济南 250031,中国兵器工业集团第五三研究所, 山东 济南 250031,中国兵器工业集团第五三研究所, 山东 济南 250031,中国兵器工业集团第五三研究所, 山东 济南 250031,中国兵器工业集团第五三研究所, 山东 济南 250031 |
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| 摘 要： | 用气相色谱/质谱法(GC/MS)分析了4种航空燃料JP-10的成分。研究了色谱的线性范围。用外标法测定了JP-10燃料的纯度。结果表明,航天燃料JP-10中除了主体成分外式-四氢双环戊二烯,还有十氢萘、內式-四氢双环戊二烯、金刚烷及它们的甲基化产物等杂质。外标法定量适宜的浓度范围为0.5~20 mg·m L-1。外标法定量可靠,准确,可用于JP-10的纯度测定。
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| 关 键 词： | 气相色谱/质谱(GC/MS) JP-10(外式-四氢双环戊二烯) 成分分析 纯度测定 |
| 收稿时间： | 2014/6/27 0:00:00 |
| 修稿时间： | 9/9/2014 12:00:00 AM |
Determination of the Composition and Purity of JP-10 by Gas Chromatography/Mass Spectrometry |
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| LI Yan-ling,JI Ke-jian,LIU Yuan-jun,GAO Di,GAO Yan-li and ZHAO Xiao-gang.Determination of the Composition and Purity of JP-10 by Gas Chromatography/Mass Spectrometry[J].Chinese Journal of Energetic Materials,2015,23(8):776-780. |
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| Authors: | LI Yan-ling JI Ke-jian LIU Yuan-jun GAO Di GAO Yan-li and ZHAO Xiao-gang |
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| Affiliation: | Institute 53 of China North Industries Group Corporation, Jinan 250031, China,Institute 53 of China North Industries Group Corporation, Jinan 250031, China,Institute 53 of China North Industries Group Corporation, Jinan 250031, China,Institute 53 of China North Industries Group Corporation, Jinan 250031, China,Institute 53 of China North Industries Group Corporation, Jinan 250031, China and Institute 53 of China North Industries Group Corporation, Jinan 250031, China |
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| Abstract: | The components of four kinds of JP-10 aviation fuels were analyzed by gas chromatography/mass spectrometry (GC/MS). The linear scope of gas chromatography was researched. The purities of JP-10 fuels were measured with an external standard method. Results show that JP-10 aviation fuels contains not only the main component exo-tetrahydrobicyclopentadiene, but also decahydronaphthalene, endo-tetrahydrobicyclopentadiene, adamantane and their methylated products, etc. The suitable concentration range for external standard method to measure the purity of JP-10 is 0.5-20 mg·mL-1. This method is reliable, accurate, and can be used for determining the purity of JP-10. |
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| Keywords: | gas chromatography/mass spectrometry JP-10(exo-THDCPD) component analysis purity determination |
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