| HPLC法测定橡胶填充油中稠环芳烃含量的研究 |
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| 引用本文： | 郑慧,齐邦峰,程仲芊,王亚婷,王兆金. HPLC法测定橡胶填充油中稠环芳烃含量的研究[J]. 化工科技, 2011, 19(2): 34-37 |
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| 作者姓名： | 郑慧 齐邦峰 程仲芊 王亚婷 王兆金 |
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| 作者单位： | 1. 辽宁石油化工大学,石油化工学院,辽宁,抚顺,113001
2. 抚顺石油化工研究院,辽宁,抚顺,113001 |
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| 摘 要： | 建立了橡胶填充油中16种优控多环芳烃(PAHs)的高效液相色谱(二极管阵列检测器HPLC)测定方法,探讨了样品的提取、固相萃取净化等前处理方法,同时也对HPLC的仪器测定条件进行了优化.在优化的条件下,16种多环芳烃化合物的平均回收率为60.4%～109.8%.方法的检测限0.49～4.32μg/L.结果表明,在检测橡...
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| 关 键 词： | 橡胶填充油 多环芳烃 HPLC |
Research on the content of polycyclic aromatic hydrocarbons in rubber filling oil by HPLC |
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| ZHENG Hui,QI Bang-feng,CHENG Zhong-qian,WANG Ya-ting,WANG Zhao-jin. Research on the content of polycyclic aromatic hydrocarbons in rubber filling oil by HPLC[J]. Science & Technology In Chemical Industry, 2011, 19(2): 34-37 |
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| Authors: | ZHENG Hui QI Bang-feng CHENG Zhong-qian WANG Ya-ting WANG Zhao-jin |
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| Affiliation: | 1.College of Petrochemical Technology,Liaoning Shihua University,Fushun 113001,China;2.Fushun Research Institute of Petroleum and Petrochemicals,Fushun 113001,China) |
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| Abstract: | A method for 16 polycyclic aromatic hydrocarbons（PAHs） in the rubber filling oil by high performance liquid chromatography（HPLC） with diode array detector has been developed.Studied on sample extraction,solid phase extraction and other pretreatment methods,and also optimized the determination conditions of HPLC.Under the optimized conditions,the average recovery of PAHs was in the range of 60.4%~109.8%.The detection limits were in the range of 0.49~4.32μg/L.The results indicated that the recoveries and detection limits of the method all reached satisfactory levels. |
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| Keywords: | HPLC |
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