| 4-氨基-6-特丁基-3-巯基-1,2,4-三嗪-5(4H)-酮高效液相色谱定量分析方法 |
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| 引用本文： | 隋志远,刘志勇,程威,吴莹,姚杰. 4-氨基-6-特丁基-3-巯基-1,2,4-三嗪-5(4H)-酮高效液相色谱定量分析方法[J]. 现代农药, 2012, 0(6): 25-26 |
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| 作者姓名： | 隋志远 刘志勇 程威 吴莹 姚杰 |
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| 作者单位： | 江苏剑牌农化股份有限公司 |
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| 摘 要： | 建立了一种采用高效液相色谱法测定4-氨基-6-特丁基-3-巯基-1,2,4-三嗪-5(4H)-酮含量的分析方法。采用C18色谱柱,以乙腈+水(体积比为2∶3)为流动相,流速为1.0 mL/min,柱温为28℃,检测波长为285 nm。方法的线性相关系数为1.0000,标准偏差为0.1389,平均回收率为99.70%。方法具有简便、快速、分离效果好、精密度和准确度高、线性相关性好的特点。
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| 关 键 词： | 4-氨基-6-特丁基-3-巯基-1,2,4-三嗪-5(4H)-酮 高效液相色谱 定量分析方法 |
Quantitative Analysis Method of 4-Amino-6-tert-butyl-3-thiol-1,2,4-triazin-5(4H)-one by HPLC |
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| SUI Zhi-yuan,LIU Zhi-yong,CHENG Wei,WU Ying,YAO Jie. Quantitative Analysis Method of 4-Amino-6-tert-butyl-3-thiol-1,2,4-triazin-5(4H)-one by HPLC[J]. Modern Agrochemicals, 2012, 0(6): 25-26 |
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| Authors: | SUI Zhi-yuan LIU Zhi-yong CHENG Wei WU Ying YAO Jie |
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| Affiliation: | (Jiangsu Sword Agrochemicals Co.,Ltd.,Jiangsu Jianhu 224700,China) |
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| Abstract: | A quantitative analysis method of 4-amino-6-tert-butyl-3-thiol-1,2,4-triazin-5（4H）-one was developed by HPLC using acetonitrile and water（V/V=2∶3） as mobile phase with a flow rate of 1.0 mL/min.A C18 column was used with the column temperature of 28℃ and the detection wavelength was 285 nm.The linear correlation coefficient was 1.0000,the standard deviation was 0.1389,and the average recovery was 99.70%.The method was convenient,fast and accurate with good separation and linear correlation. |
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| Keywords: | 4-amino-6-tert-butyl-3-thiol-1 2 4-triazin-5（4H）-one HPLC quantitative analysis method |
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