Novel Synthesis of a New Surfactant 4-((4-Bromophenyl)(dodecyl)amino)-4-Oxobutanoic Acid Containing a Benzene Ring Using a Copper Catalyst Cross-Coupling Reaction and its Properties |
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| Authors: | Minggui Chen Xinqi Hu Meilong Fu |
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| Affiliation: | 1. Key Laboratory for Oil and Gas Drilling and Production Engineering of Hubei Province, College of Petroleum Engineering, Yangtze University, Jingzhou, 434023, People’s Republic of China
2. College of Chemistry and Chemical Engineering, Southwest Petroleum University, Chengdu, 610500, People’s Republic of China
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| Abstract: | A new surfactant 4-((4-bromophenyl)(dodecyl)amino)-4-oxobutanoic acid with a benzene spacer was synthesized via a novel copper catalyzed cross-coupling reaction. Its structure was confirmed by FTIR, 1H-NMR, 13C-NMR and HRMS; its purity was checked by HPLC. Dynamic light scattering and an atomic force microscope showed that it forms an unusual large-diameter premicellar aggregation below the CMC. |
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| Keywords: | Surfactant with benzene ring Cross‐coupling reaction Synthesis Property |
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