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水萃取法测定纺织品甲醛含量不确定度的评定
引用本文:高小兰,蚁乐洲,刘伟红.水萃取法测定纺织品甲醛含量不确定度的评定[J].广东化工,2014(11):207-208,212.
作者姓名:高小兰  蚁乐洲  刘伟红
作者单位:广东出入境检验检疫局检验检疫技术中心,广东广州510623
摘    要:文章评定了GB 18401-2010《国家纺织产品基本安全技术规范》中三类纺织品服装的游离甲醛限量的相对不确定度和扩展不确定度。建立纺织品甲醛含量不确定度的数学模型,系统分析计算不确定度的各个分量1]。按GB/T 2912.1-2009《纺织品甲醛的测定第1部分:游离和水解甲醛(水萃取法)》测定了三类纺织品中的甲醛含量,其扩展不确定度分别为2.0 mg/kg、4.0 mg/kg、13.0 mg/kg。当样品甲醛的含量在限量附近时,用不确定度校正后的结果更可靠和准确。

关 键 词:纺织品甲醛  不确定度  水萃取法

The Evaluation of Uncertainty of Formaldehyde Content in Textiles Determined by Water Extraction Method
Gao Xiaolan,Yi Lezhou,Liu Weihong.The Evaluation of Uncertainty of Formaldehyde Content in Textiles Determined by Water Extraction Method[J].Guangdong Chemical Industry,2014(11):207-208,212.
Authors:Gao Xiaolan  Yi Lezhou  Liu Weihong
Affiliation:(Guangdong Inspection and Quarantine Technology Center, Guangzhou 510623, China)
Abstract:The relative uncertainty and expanded uncertainty of limited amount of formaldehyde in three categories of textiles and clothing provided by GB 18401-2010, (National General Technical Code for Textile Products) were evaluated. Mathematical mode of the uncertainty of formaldehyde in textiles was established and each component of the uncertainty was analyzed and calculated systematically. Formaldehyde contents in three categories of textiles were determined in accordance with GB/T 2912.1-2009, Determination of Formaldehyde in Textiles, Part I: Free and Hydrolyzed Formaldehyde(Water Extraction Method) and the corresponding expanded uncertainty is 2.0 mg/kg, 4.0 mg/kg, 13.0 mg/kg respectively. It is more accurate and reliable to analyze data with uncertainty when the content of sample is close to the limited amount.
Keywords:formaldehyde in textiles  the uncertainty  water extraction method
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