| 2-叔丁氨甲基-2-硝基-l,3-丙二醇盐酸盐的合成与表征 |
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| 引用本文： | 杨佳理,;解秋莲,;刘愆,;李健康,;李陶琦. 2-叔丁氨甲基-2-硝基-l,3-丙二醇盐酸盐的合成与表征[J]. 广东化工, 2014, 0(13): 114-115 |
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| 作者姓名： | 杨佳理, 解秋莲, 刘愆, 李健康, 李陶琦 |
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| 作者单位： | [1]陕西国防工业职业技术学院,陕西西安710302; [2]西安近代化学研究所,陕西西安710065 |
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| 摘 要： | 以3-叔丁基-5-羟甲基-5-硝基四氢-l,3-噁嗪为原料,以水为溶剂,经酸性水解合成了2-叔丁氨甲基-2-硝基-l,3-丙二醇盐酸盐,并对其结构进行了红外光谱、核磁共振波谱和元素分析表征。
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| 关 键 词： | -叔丁氨甲基--硝基-l -丙二醇盐酸盐 水解 表征 |
Synthesis and Characterization of 2-tert-butylaminomethyl-2-nityl-1,3-propanediol hydrochloride |
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| Affiliation: | Yang Jiali, Xie Qiulian, Liu Qian, Li Jiankang, Li Taoqi. (1. Shaanxi Institute of Technology, Xi＇an 710300; 2. Xi＇an Modem Chemistry Research Institute, Xi＇ an 710065, China) |
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| Abstract: | 2-Tert-butylaminamethyl-2-nityl-1,3-propanediol hydrochloride was synthesized with 3-tert-butyl-5-nitro-tetrahydro-1,3（4H）-oxazine as materials, water as solvent by acid hydrolysis, the product was characterized by IR, HNMR, CNMR and element analysis. The result shows that the structure characteristics of product is accorded with 2-tert-butylaminamethyl-2-nityl-1,3-propanediol hydrochloride. |
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| Keywords: | 2-tert-butylaminamethyl-2-nityl-1,3-propanediolhydrochloride synthesis characterization |
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