| 1-苄基-4-（4-甲氧基）-苯基-1，2，3-三唑的合成 |
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| 引用本文： | 陈刚,顾雪凡,孟梅,汤颖. 1-苄基-4-（4-甲氧基）-苯基-1，2，3-三唑的合成[J]. 广州化工, 2009, 37(1): 84-84 |
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| 作者姓名： | 陈刚 顾雪凡 孟梅 汤颖 |
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| 作者单位： | 西安石油大学化学化工学院,陕西,西安,710065 |
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| 摘 要： | 采用氯苄和叠氮化钠在乙醇中反应制备了苄叠氮，进而与对甲氧基苯乙炔进行1，3-偶极环加成反应合成了未见报道的1-苄基-4-（4-甲氧基）-苯基-1，2，3-三唑，产率达到了48％，产物结构经NMR和MS确认。
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| 关 键 词： | 三唑 环加成反应 合成 |
Preparation of 1-Benzyl-4-(4-Methyloxy)Phenyl-1, 2, 3-Triazole |
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| CHEN Gang,GU Xue-fan,MENG Mei,TANG Ying. Preparation of 1-Benzyl-4-(4-Methyloxy)Phenyl-1, 2, 3-Triazole[J]. GuangZhou Chemical Industry and Technology, 2009, 37(1): 84-84 |
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| Authors: | CHEN Gang GU Xue-fan MENG Mei TANG Ying |
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| Affiliation: | College of Chemistry and Chemical Engineering;Xi'an Shi You University;Shanxi Xi'an 701165;China |
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| Abstract: | Benzyl azide was synthesized in ethyl alcohol by substitution reaction with benzyl chloride and sodium azide,and then 1-benzyl-4-(4-methyloxy)phenyl-1,2,3-triazole was prepared by 1,3-dipolar cycloaddition of benzyl azide and 4-methoxyphenylacetylene,with the yield of 48 %.The structures of the products were characterized by NMR and MS. |
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| Keywords: | triazole 1 3-dipolar cycloaddition synthesis |
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