| 三氯氢硅气相色谱分析条件研究 |
| |
| 引用本文： | 杨裴,范国强,白莹,郭永欣,胡家啟,叶世胜. 三氯氢硅气相色谱分析条件研究[J]. 无机盐工业, 2012, 44(9): 51-53 |
| |
| 作者姓名： | 杨裴 范国强 白莹 郭永欣 胡家啟 叶世胜 |
| |
| 作者单位： | 1.中海油天津化工研究设计院，天津 300131；2.浙江新安化工有限公司 |
| |
| 摘 要： | 对三氯氢硅气相色谱分析条件进行了研究，确定了三氯氢硅毛细管柱的色谱分析条件。采用确定的色谱分析条件进行了方法的线性范围测定，得到线性相关系数R=0.999 93。进行了方法的平行性和重复性试验，结果表明：方法的平行性好，重复性好，三氯氢硅质量分数的相对标准偏差（RSD）小于0.02%，结果令人满意。
|
| 关 键 词： | 三氯氢硅 气相色谱法 毛细管柱 |
Study on quantitative GC analysis conditions for trichlorosilane |
| |
| Yang Pei , Fan Guoqiang , Bai Ying , Guo Yongxin , Hu Jiaqi , Ye Shisheng. Study on quantitative GC analysis conditions for trichlorosilane[J]. Inorganic Chemicals Industry, 2012, 44(9): 51-53 |
| |
| Authors: | Yang Pei Fan Guoqiang Bai Ying Guo Yongxin Hu Jiaqi Ye Shisheng |
| |
| Affiliation: | 1.CNOOC Tianjin Chemical Research & Design Institute，Tianjin 300131；2.Zhejiang Xin′an Chemical Industry Group Co.,Ltd. |
| |
| Abstract: | Analysis conditions of trichlorosilane by gas chromatography were studied,and the optimum analysis conditions of gas chromatography with capillary column for trichlorosilane were comfirmed.The liner range of this analysis method was determined with the defined analysis conditions,and linear correlation was obtained,i.e.R=0.999 93.Parallel and repeated tests were also carried out and results showed the method had good parallelity and repeatability.The relative standard deviation(RSD) of the mass fraction of trichlorosilane was less than 0.02% and the result was satisfied. |
| |
| Keywords: | trichlorosilane gas chromatography capillary column |
| 本文献已被 CNKI 万方数据 等数据库收录！ |
| 点击此处可从《无机盐工业》浏览原始摘要信息 |
|
点击此处可从《无机盐工业》下载全文 |
