| 纳米MoS2的制备及其与聚吡咯物复合膜光学性能的研究 |
| |
| 引用本文： | 何晓云,钟淮真,李国强,陈力勤,陈震.纳米MoS2的制备及其与聚吡咯物复合膜光学性能的研究[J].化学世界,2006,47(2):69-70,77. |
| |
| 作者姓名： | 何晓云 钟淮真 李国强 陈力勤 陈震 |
| |
| 作者单位： | 福建师范大学化学与材料学院,福建,福州,350007 |
| |
| 基金项目： | 福建省科技厅重点项目(02H034)，福建省教育厅项目(JA02192,JA02189,JB02177) |
| |
| 摘 要： | 以有机热溶剂法制备MoS2,并以XRD对其结构进行表征.TEM形貌观察表明晶粒具有纳米尺寸。以电化方法在ITO导电玻璃基体上制备聚合物聚吡咯薄膜。在导电聚合物膜上涂布纳米MoS2晶体,荧光分析发现其荧光光谱相对于聚合物膜有一定程度的红移。Z-Scan测试其折射率的结果表明其具有非线性光学特性。
|
| 关 键 词： | 聚吡咯 复合膜 纳米 半导体 |
| 文章编号： | 0367-6358（2006）02-69-03 |
| 收稿时间： | 2004-12-01 |
| 修稿时间： | 2004-12-012005-12-09 |
Study on the Preparation of Nanosize MoS2 and Photo Characteristics of MoS2-polyconductor Film |
| |
| HE Xiao-yun,ZHONG Huai-zhen,LI Guo-qiang,CHEN Li-qin,CHEN Zhen.Study on the Preparation of Nanosize MoS2 and Photo Characteristics of MoS2-polyconductor Film[J].Chemical World,2006,47(2):69-70,77. |
| |
| Authors: | HE Xiao-yun ZHONG Huai-zhen LI Guo-qiang CHEN Li-qin CHEN Zhen |
| |
| Affiliation: | College of Chemistry and Materials Science, Fujian Normal University, Fujian Fuzhou 350007, China |
| |
| Abstract: | Nanosize MoS_2 semiconductor particles were synthesized by using the solvothermal technique.The structure was characterized by means of XRD,TEM techniques.PPY films were prepared by electro-chemical method onto the indium-tin oxide glass(ITO).The nanoparticles were doped on the polyconductor film by the dipping process,and the nanoparticle-polyconductor composite films were acquired.The optical properties of the films were studied by PL method.The red shift in the fluorescence spectra for the nanocrystal-polyconductor composite films was observed.The refractive index of the films was obtained by Z-Scan,and the result indicated the films possessed nonlinear photo characteristics. |
| |
| Keywords: | polypyrrole composition film nanoparticle semiconductor |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
