| 催化精馏法制备丙二醇单乙醚的中型试验 |
| |
| 引用本文： | 于洪涛.催化精馏法制备丙二醇单乙醚的中型试验[J].精细石油化工,2002(3):56-59. |
| |
| 作者姓名： | 于洪涛 |
| |
| 作者单位： | 中石化股份有限公司天津分公司,天津,300271 |
| |
| 摘 要： | 考察了环氧丙烷 (PO)和乙醇在新型 β沸石分子筛催化剂存在下 ,应用催化精馏法制备丙二醇乙醚的中型试验 ,PO为 2 2 .5kg/h ,乙醇为 15 0～ 180kg/h(新鲜加馏出 ) ,β沸石催化剂装填量为 4 0kg ,反应温度为(10 5± 5 )℃ ,塔底温度为 170～ 175℃ ,系统压力为 0 .15～ 0 .17MPa ,丙二醇单乙醚收率为 90 .5 %。确定了该生产方法的工艺条件。
|
| 关 键 词： | 丙二醇单乙醚 催化精馏 制备 新型β沸石 催化剂 |
| 修稿时间： | 2002年1月5日 |
PILOT PLANT TESTS ON PREPARATION OF PROPYLENE GLYCOL MONO ETHYL ETHER BYCATALYTIC DISTILLATION PROCESS |
| |
| Yu Hongtao.PILOT PLANT TESTS ON PREPARATION OF PROPYLENE GLYCOL MONO ETHYL ETHER BYCATALYTIC DISTILLATION PROCESS[J].Speciality Petrochemicals,2002(3):56-59. |
| |
| Authors: | Yu Hongtao |
| |
| Abstract: | The pilot plant tests of catalytic distillation for preparing propylene glycol mono ethyl ether from propylene oxide (PO) and ethanol in presence of a β zeolite molecular sieve catalyst were investigated. The technogical conditions were established as follows: PO feeding rate 22.5 kg/h, ethanol feeding rate 150180 kg/h (fresh plus recovered), catalyst charge amount 40 kg, reaction temperature (105±5) ℃, tower bottom temperature 170175 ℃, system pressure 0.150.17 MPa. The yield of propylene glycol mono ethyl ether was 90.5%. |
| |
| Keywords: | propylene glycol mono ethyl ether catalytic distillation preparation β zeolite molecular sieve catalyst pilot plant test |
| 本文献已被 CNKI 万方数据 等数据库收录！ |
|
