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8-羟基喹啉重量法测定钨精矿中WO_3的含量
引用本文:吴伟明,徐晶,梁晓鹏,柴敏平,程明焱,蒋小岗. 8-羟基喹啉重量法测定钨精矿中WO_3的含量[J]. 中国钨业, 2012, 27(3): 36-39
作者姓名:吴伟明  徐晶  梁晓鹏  柴敏平  程明焱  蒋小岗
作者单位:1. 江西理工大学,江西赣州,341000
2. 国家钨与稀土产品质量监督检验中心,江西赣州,341000
基金项目:国家质量监督检验检疫总局科技计划质量监督项目(2011QK219)
摘    要:对钨精矿中钨含量测定的常用重量法进行了综合评述;对8-羟基喹啉重量法中硫-磷混酸分解试样条件、沉淀条件选择及干扰元素影响的消除、最佳显色条件等进行实验探讨。结果表明,试样分解快速完全、结果精密度高、方法可行有效。

关 键 词:  8-羟基喹啉  重量法

Determining WO3 Content in Tungsten Concentrate by 8-Hydroxyquinoline Gravimetric Method
WU Wei-ming , XU Jing , LIANG Xiao-peng , CHAI Min-ping , CHENG Ming-yan , JIANG Xiao-gang. Determining WO3 Content in Tungsten Concentrate by 8-Hydroxyquinoline Gravimetric Method[J]. China Tungsten Industry, 2012, 27(3): 36-39
Authors:WU Wei-ming    XU Jing    LIANG Xiao-peng    CHAI Min-ping    CHENG Ming-yan    JIANG Xiao-gang
Affiliation:WU Wei-ming, XU Jing, LIA NG Xiao-peng, CHAI Min-ping, CHENG Ming-yan, JIA NG Xiao-gang (1.Jiangxi University of Science and Technology, Ganzhou 341000, Jiangxi, China; 2.China Quality Supervision and Inspection Center of Tungsten and Rare- earth Products, Ganzhou 341000, Jiangxi, China)
Abstract:This article reviews the advantages and disadvantages of the common gravimetric methods for the content determination of tungsten. The conditions of decomposition and precipitation of the 8-hydroxyquinoline gravimetric method to determine WO3 content in tungsten concentrate were studied by stating the best conditions of color reaction. The experimental results show that the sample decomposition is fast and complete, which shows the method is accurate, convenient and efficient.
Keywords:tungsten  8-hydroxyquinoline  gravimetric method
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