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Solubility Limit of MgO in Al2O3 at 1600°C
Authors:Lior Miller  Amir Avishai   Wayne D. Kaplan
Affiliation:Department of Materials Engineering, Technion-Israel Institute of Technology, Haifa 32000, Israel
Abstract:The solubility of Mg in alumina was measured using wavelength-dispersive spectroscopy mounted on a scanning electron microscope. Careful calibration of the microscope's working conditions was performed in order to optimize the detection limit and accuracy. Measurements were conducted on water-quenched and furnace-cooled samples, without any thermal or chemical etching to avoid alteration of the bulk concentration. The results indicate the solubility limit of Mg in alumina to be 132±11 ppm at 1600°C.
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