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Influence of the sintering conditions on the physical proprieties of the ceramic PFN multiferroics
Authors:Dariusz Bochenek  Zygmunt Surowiak  Józef Krok-Kowalski  Jana Poltierova-Vejpravova
Affiliation:1. Department of Materials Science, University of Silesia, 2, ?nie?na St., Sosnowiec, 41-200, Poland
2. Institute of Physics, University of Silesia, 14, Uniwersytecka St., Katowice, 40-007, Poland
3. Department of Condensed Matter Physics, Charles University, Ke Karlovu 5, 121 16, Praha 2, The Czech Republic
Abstract:An influence of compacting conditions on applied properties of the multiferroic PbFe1/2Nb1/2O3 (PFN) ceramics synthesized by the columbite method and powder calcination technique is presented in this work. The obtained specimens were subjected to X-ray and chemical composition homogeneity analyses, magnetic tests, electric direct current conductivity and electromechanical tests. Differences in the degree of diffuseness, densities and a grain size were observed depending on the sintering method. The dielectric and magnetic parameters as a function of temperature were measured. The tests confirmed that PFN powder compacting by a hot uniaxial pressing method had an advantageous influence on the crystalline structure ordering and the ceramics microstructure, what improves the applied properties of the material.
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