| 消痈喷雾剂提取工艺研究 |
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| 引用本文： | 李本俊,薛霞,王立池,徐冬雨.消痈喷雾剂提取工艺研究[J].辽宁化工,2014(11):1367-1369,1372. |
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| 作者姓名： | 李本俊 薛霞 王立池 徐冬雨 |
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| 作者单位： | 辽宁医药职业学院;辽宁中医药大学;大连鹏润医药有限公司 |
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| 摘 要： | 研究了消痈喷雾剂的乙醇最佳提取工艺。采用正交试验,以黄芩苷提取量为考察指标,优选消痈喷雾剂最佳提取工艺。实验结果显示最佳工艺条件是60%乙醇溶液,10,8,8倍溶媒量,提取2 h,提取3次。优选得到的工艺稳定可行,适合工业化大生产。
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| 关 键 词： | 黄芩苷 提取工艺 正交设计 含量测定 高效液相 |
Optimization of Extracting Process Conditions of Xiaoyong Spray by Orthogonal Test |
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| LI Ben-jun;XUE Xia;WANG Li-chi;XU Dong-yu.Optimization of Extracting Process Conditions of Xiaoyong Spray by Orthogonal Test[J].Liaoning Chemical Industry,2014(11):1367-1369,1372. |
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| Authors: | LI Ben-jun;XUE Xia;WANG Li-chi;XU Dong-yu |
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| Affiliation: | LI Ben-jun;XUE Xia;WANG Li-chi;XU Dong-yu;Liaoning Medicine Vocational College;Liaoning University of Traditional Chinese Medicine;.Dalian Pengrun Medicine Co.,Ltd.; |
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| Abstract: | To study optimum extraction process conditions for Xiaoyong spray, the orthogonal design was carried out. The processconditions were optimized by determining the utilization ratio of baicalin.The results show that the optimum extraction conditions areas follows： 60% alcohol, amount of alcohol 10, 8,8 times, extraction times 3, extraction time 2 h. The optimized process is stable andsuitable for industrial production. |
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| Keywords: | baicalin extraction process orthogonal design detelTnination high performance liquid chromatography |
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