| 糠酸甲酯的合成 |
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| 引用本文： | 郑静,刘咏琴,吕佳月. 糠酸甲酯的合成[J]. 精细化工中间体, 2007, 37(1): 41-42,45 |
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| 作者姓名： | 郑静 刘咏琴 吕佳月 |
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| 作者单位： | 湖北师范学院,化学与环境工程系,湖北,黄石,435002;湖北师范学院,化学与环境工程系,湖北,黄石,435002;湖北师范学院,化学与环境工程系,湖北,黄石,435002 |
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| 摘 要： | 以糠醛为起始原料,通过康尼查罗反应、酰氯化和酯化反应合成了糠酸甲酯,实验结果表明:酯化反应时间2.5h,糠酸甲酯收率可达85.0%。
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| 关 键 词： | 糠酸甲酯 糠醛 二氯亚砜 康尼查罗反应 酯化 |
| 文章编号： | 1009-9212（2007）01-0041-02 |
| 修稿时间： | 2006-10-20 |
Synthesis of Methyl-furoate |
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| ZHENG Jing,LIU Yong-qin,L Jia-yue. Synthesis of Methyl-furoate[J]. Fine Chemical Intermediates, 2007, 37(1): 41-42,45 |
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| Authors: | ZHENG Jing LIU Yong-qin L Jia-yue |
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| Affiliation: | Department of Chemistry and Environmental Engineering, Hubei Normal University, Huangshi 435002, China |
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| Abstract: | Methyl-furoate is synthesized from furfural by Cannizzaro reaction, acyl chloride reaction and esterification. It showed that the time of esterification is only 2.5 hours and the yield can reach 85.0%. |
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| Keywords: | methyl-furoate furfural sulfuryl dichloride cannizzaro reaction esterification |
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