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气相色谱法测定早强剂中的三乙醇胺
引用本文:张丹青,郑建明,肖时俊,黄龙娣.气相色谱法测定早强剂中的三乙醇胺[J].山东化工,2011,40(4):44-46.
作者姓名:张丹青  郑建明  肖时俊  黄龙娣
作者单位:江苏天瑞仪器股份有限公司,江苏,苏州,215300
摘    要:建立了气相色谱法测定早强剂中三乙醇胺的方法。本方法的相对标准偏差(RSD)≤2.32%,回收率在93.5%~103.7%,三乙醇胺的方法检出限为0.5mg/kg,是首次采用气相色谱仪对水泥早强剂中的三乙醇胺进行分析的一种方法。

关 键 词:气相色谱  三乙醇胺  水泥早强剂

Determination of Triethanolamine in Early Strength Agent by Gas Chromatography
ZHANG Dan-qing,ZHENG Jian-ming,XIAO Shi-jun,HUANG Long-di.Determination of Triethanolamine in Early Strength Agent by Gas Chromatography[J].Shandong Chemical Industry,2011,40(4):44-46.
Authors:ZHANG Dan-qing  ZHENG Jian-ming  XIAO Shi-jun  HUANG Long-di
Affiliation:ZHANG Dan - qing , ZHENG Jian - ruing, XIAO Shi -jun, HUANG Long - di (Jiangsu Skyray Instrument Co. , Ltd. , Suzhou 215300,China)
Abstract:Established the method of determination for triethanolamine in early strength agent by gas chromatography. The relative standard deviati6n (RSD) for this method was ≤ 2.32%, recovery between 93.5% - 103.7%, triethanolamine detection limit was 0. 5mg/kg. This method is applicable to the cement thickening in the analysis of triethanolamine using gas chromatography for the first time.
Keywords:gas chromatography  tfiethanolamine  cement early strength agent
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