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6-APA中残留丙酮、甲基异丁基酮的测定
引用本文:赵娜,宋雅丽,郭云英. 6-APA中残留丙酮、甲基异丁基酮的测定[J]. 河北化工, 2012, 35(7): 36-39,57
作者姓名:赵娜  宋雅丽  郭云英
作者单位:石药集团中诺药业(石家庄)有限公司,河北石家庄,050041
摘    要:采用直接进样色谱法测定,并用内标法(2-戊酮作内标物)定量,确定6-APA中残留丙酮、甲基异丁基酮的检测方法。经验证此法可准确测定6-APA中丙酮、甲基异丁基酮的残余量。

关 键 词:6-APA  丙酮  甲基异丁基酮  气相色谱法

Determination on Residual Acetone and MIBK in 6-APA
ZHAO Na,SONG Ya-li,GUO Yun-ying. Determination on Residual Acetone and MIBK in 6-APA[J]. Hebei Chemical Engineering and Industry, 2012, 35(7): 36-39,57
Authors:ZHAO Na  SONG Ya-li  GUO Yun-ying
Affiliation:(CSPC Zhongnuo Pharmaceutical(Shijiazhuang)Co.,Ltd,Shijiazhuang 050041,China)
Abstract:To develop a method for determination of residual acetone and MIBK in 6-APA through using injection chromatographic method and internal standard(2-pentanone) method.This method established on basis of verification to determinate residual acetone and MIBK in 6-APA accurately.
Keywords:6 -APA  acetone  MIBK  gas chromatography method
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