| 杂多酸(盐)催化新型香料草莓酯的合成 |
| |
| 引用本文： | 刘杰凤,农兰平,蒋维. 杂多酸(盐)催化新型香料草莓酯的合成[J]. 精细化工中间体, 2003, 33(3): 19-20,41 |
| |
| 作者姓名： | 刘杰凤 农兰平 蒋维 |
| |
| 作者单位： | 茂名学院,广东 茂名,525000 |
| |
| 摘 要： | 采用硅钨酸铝作催化剂 ,以乙酰乙酸乙酯和 1 ,2 丙二醇为原料合成草莓酯。优化的反应条件为 :0 2mol乙酰乙酸乙酯 ,0 2mol1 ,2 丙二醇 ,40ml环己烷 ,0 3 g硅钨酸铝 ,反应 3 5h ,草莓酯收率达 81 6%。产物经理化检验和红外光谱确证
|
| 关 键 词： | 草莓酯 杂多酸 合成 |
| 文章编号： | 1009-9212(2003)03-0019-02 |
Synthesis of a New Type Perfume Fraistone Catalyzed by Heteropoly Acids(salt) |
| |
| LIU Jie feng etc.. Synthesis of a New Type Perfume Fraistone Catalyzed by Heteropoly Acids(salt)[J]. Fine Chemical Intermediates, 2003, 33(3): 19-20,41 |
| |
| Authors: | LIU Jie feng etc. |
| |
| Abstract: | Fraistone was synthesized with reaction of Ehyl Acetyl acetate and 1,2 Propanediol, by aluminnm silicolungstie as catatlyst. The optimum conditions are follows: the ratio of ethyl acetate, 1,2 Propanediol, Cyclohexane,Aluminnm Silicolungstie is 0.2?mol:0.2?mol:40?ml:0.3?g, reaction for 3.5 hours.The yield reaches 81.6%. The product was characterized by the physical and chemical character, and spectra. |
| |
| Keywords: | fraistone heteropoly acids synthesis |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
