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原位观察镍基高温合金CMSX-4缩松形成过程及机理研究
引用本文:许桐舟,潘秀红,张明辉,汤美波,李会东,刘学超. 原位观察镍基高温合金CMSX-4缩松形成过程及机理研究[J]. 稀有金属材料与工程, 2021, 50(4): 1113-1117
作者姓名:许桐舟  潘秀红  张明辉  汤美波  李会东  刘学超
作者单位:中国科学院上海硅酸盐研究所 上海,中国科学院上海硅酸盐研究所 上海,中国科学院上海硅酸盐研究所 上海,中国科学院上海硅酸盐研究所 上海,中国科学院上海硅酸盐研究所 上海,中国科学院上海硅酸盐研究所 上海
基金项目:上海市重大科技公关项目19DZ1100703;国家自然科学基金NO.51472263; 中科院上硅所提前启动基金Y82ZC8180G;中科院太空制造重点实验室自主课题SMT-2019-004
摘    要:采用共聚焦激光扫描显微镜(CLSM)对镍基单晶高温合金CMSX-4的凝固行为进行实时观察.并利用扫描电镜(SEM)和能谱仪(EDS)对凝固样品的微观形貌和元素偏析特性进行研究.结果 表明,在合金凝固过程中观察到缩松和碳化物的形成.缩松具有3种形态:方形缩松,五角星形缩松和角形缩松.并讨论了3种缩松的形成机理,缩松的形成...

关 键 词:原位观察  CMSX-4  缩松  碳化物  凝固机理
收稿时间:2020-08-13
修稿时间:2020-11-05

In-situ Observation of Shrinkage Formation and Mechanism during Ni-based Superalloy Solidification
Tongzhou Xu,Xiuhong Pan,Minghui Zhang,Meibo Tang,Huidong Li and Xuechao Liu. In-situ Observation of Shrinkage Formation and Mechanism during Ni-based Superalloy Solidification[J]. Rare Metal Materials and Engineering, 2021, 50(4): 1113-1117
Authors:Tongzhou Xu  Xiuhong Pan  Minghui Zhang  Meibo Tang  Huidong Li  Xuechao Liu
Affiliation:Shanghai Institute of Ceramics,Chinese Academy of Sciences,Shanghai Institute of Ceramics,Chinese Academy of Sciences,Shanghai Institute of Ceramics,Chinese Academy of Sciences,Shanghai Institute of Ceramics,Chinese Academy of Sciences,Shanghai Institute of Ceramics,Chinese Academy of Sciences,Shanghai Institute of Ceramics,Chinese Academy of Sciences
Abstract:Confocal laser scanning microscope(CLSM) was used to observe the solidification behavior of Nickel-based single crystal superalloy CMSX-4 in real time. SEM and EDS were used to study the micromorphology and element segregation characteristics of the solidified samples. Shrinkage and carbide formation were observed during alloy solidification. There are three types of shrinkages: square shrinkages, pentagonal star shrinkages and angular shrinkages. The formation mechanism of the three shrinkages is disccused, which is mainly related to the shape of the enclosed area surrounded by the secondary dendrite arms growing in different directions. In addition, carbides are found to be composed of two forms, namely flocculent carbide and lath carbide. Hf elements are enriched in flocculent carbides, while Cr elements are enriched in lath carbides.
Keywords:In situ observation   CMSX-4   shrinkage   carbide   solidification mechanism
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