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Preparation of nanosized synthetic rutile from ilmenite concentrate
Authors:BN Akhgar  M Pazouki  M Ranjbar  A Hosseinnia  M Keyanpour-Rad
Affiliation:1. Department of Mineral Processing, Engineering Faculty, Shahid Bahonar University, Kerman, Iran;2. Materials and Energy Research Center, MeshkinDasht, Karaj, Iran;1. School of Resources and Civil Engineering, Northeastern University, Shenyang 110819, Liaoning, PR China;2. BGRIMM Technology Group, Beijing 100160, PR China;1. Department of Chemistry, University of Ilorin, P. M. B. 1515, Ilorin 240003, Nigeria;2. Hydro & Electrometallurgy Department, CSIR-Institute of Minerals and Materials Technology, Bhubaneswa 751013, India;3. CSIR-Central Road Research Institute, New Delhi 110025, India;1. Division of Mineral Processing Engineering, Institute of Processing Engineering, Chinese Academy of Sciences, Beijing 100190, China;2. University of Chinese Academy of Sciences, Beijing 100049, China;1. School of Engineering, The University of Edinburgh, Edinburgh EH9 3JL, UK;2. School of Chemistry, The University of Edinburgh, Edinburgh EH9 3JL, UK
Abstract:In this paper, the preparation of nanosized synthetic rutile by reductive hydrochloric acid leaching of mechanically activated ilmenite concentrate (FeTiO3) is discussed. X-ray fluorescence analysis of the nanosized rutile which forms by rapid hydrolysis of dissolved titanium indicates that the powder contains 91.1% TiO2, 1.3% Fe2O3, 6.3% SiO2. The presence of the rutile phase is confirmed by X-ray diffractometry and the sizes of particles are measured by transmission electron microscopy to be less than 100 nm. The photocatalytic activity of nanosized rutile is observed by the decomposition of methylene blue.
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