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| 微波等离子体法合成洋葱状富勒烯的研究 | |
| 引用本文： | 符冬菊,刘旭光,杜爱兵,韩培德,贾虎生,许并社. 微波等离子体法合成洋葱状富勒烯的研究[J]. 无机材料学报, 2006, 21(3): 576-582. DOI: 10.3724/SP.J.1077.2006.00576 |
| 作者姓名： | 符冬菊 刘旭光 杜爱兵 韩培德 贾虎生 许并社 |
| 作者单位： | 1. 太原理工大学材料科学与工程学院, 太原030024; 2. 太原理工大学化学化工学院, 太原 030024 |
| 基金项目： | 科技部科研项目;国家自然科学基金;中国科学院资助项目;山西省留学基金 |
| 摘 要： | 在微波等离子体条件下, 以乙炔炭黑/二茂铁为原料, 低温合成纳米洋葱状富勒烯(Nano-structured Onion-like Fullerenes: NSOFs). 采用HRTEM、Raman和XRD等分析方法对产物的形貌、尺寸、微观结构及其物相结构进行了表征. 结果表明, 以乙炔炭黑/二茂铁为原料可大量合成NSOFs, 其外观呈准球状或多面体状、实心、直径分布均匀, 最外碳层由闭合的、呈波浪状的石墨片构成. |
| 关 键 词： | 纳米洋葱状富勒烯 微波等离子体 炭黑 |
| 文章编号： | 1000-324X（2006）03-0576-07 |
| 收稿时间： | 2005-06-13 |
| 修稿时间： | 2005-06-132005-11-21 |
Synthesis of Nano-structured Onion-like Fullerenes by MW Plasma |
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| FU Dong-Ju,LIU Xu-Guang,DU Ai-Bing,HAN Pei-De,JIA Hu-Sheng,XU Bing-She. Synthesis of Nano-structured Onion-like Fullerenes by MW Plasma[J]. Journal of Inorganic Materials, 2006, 21(3): 576-582. DOI: 10.3724/SP.J.1077.2006.00576 | |
| Authors: | FU Dong-Ju LIU Xu-Guang DU Ai-Bing HAN Pei-De JIA Hu-Sheng XU Bing-She |
| Affiliation: | 1. College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, China; 2. College of Chemistry and Chemical Engineering, Taiyuan University of Technology, Taiyuan 030024, China |
| Abstract: | Nano-structured onion-like fullerenes (NSOFs) were synthesized from C2H2 carbon black/ferrocene by microwave plasma. High resolution transmission electron microscope (HRTEM), Raman and X-ray diffraction (XRD) techniques were used to characterize the morphologies and structures of the products. Results indicated that NSOFs could be prepared from C2H2 carbon black/ferrocene. The particles displayed a clear polyhedral or spherical morphology, with cores and waving out layers. |
| Keywords: | nano-structured onion-like fullerenes microwave plasma carbon black |
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