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天山堇菜中挥发油的气相色谱-质谱分析
引用本文:沈小燕,解成喜,邓卫萍.天山堇菜中挥发油的气相色谱-质谱分析[J].质谱学报,2009,30(1):51-54.
作者姓名:沈小燕  解成喜  邓卫萍
作者单位:新疆大学理化测试中心,新疆 乌鲁木齐 830046
摘    要:为探索天山堇菜的药理活性与其挥发油化学成分的关系,用挥发油提取器提取天山堇菜中的挥发油,测得含量为0.067%。采用气相色谱-质谱联用技术对天山堇菜的挥发性成分进行分离鉴定,共分离出60种成分,确认了其中的47种成分,占挥发油总离子流的75.54%。采用峰面积归一化法确定各成分的相对百分含量,其中主要成分为脂肪烃和含氧有机化合物(醇、酮、醛和酯)。

关 键 词:气相色谱-质谱  挥发油  天山堇菜  
收稿时间:2008-05-29

Analysis of Volatile Oil from Viola Tianshanica Maxim by GC/MS
SHEN Xiao-yan,XIE Cheng-xi,DENG Wei-ping.Analysis of Volatile Oil from Viola Tianshanica Maxim by GC/MS[J].Journal of Chinese Mass Spectrometry Society,2009,30(1):51-54.
Authors:SHEN Xiao-yan  XIE Cheng-xi  DENG Wei-ping
Affiliation:Physical and Chemical Analysis Center,Xinjiang University,Urumqi 830046,China
Abstract:The chemical components of volatile oils from Viola tianshanica Maxim were analyzed by gas chromatography-mass spectrometry (GC/MS). The content of the volatile oils which were extracted by steam distillation from Viola tianshanica Maxim was 0.067%. 47 components are identified from 60 separated peaks, amounting to total mass fraction 75.54% . The relative contents of the components were determined with peak area normalization method. The major constituents of the volatile oils are aliphatic hydrocarbons, alcohols, ketone, aldehyde and esters.
Keywords:gaschromatography-massspectrometry(GC/MS)  volatileoil  ViolatianshanicaMaxim  
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