| 气相色谱-质谱法测定纺织品中的有机锡 |
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| 引用本文： | 胡志国. 气相色谱-质谱法测定纺织品中的有机锡[J]. 质谱学报, 2005, 26(1): 59-59 |
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| 作者姓名： | 胡志国 |
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| 作者单位： | 勤兴软胶厂(深圳)有限公司,广东,深圳,518132 |
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| 摘 要： | 介绍了利用酸性人工汗液萃取 ,气相色谱 -质谱联用法 (GC/ MS)测定纺织品中的可溶出有机锡 (主要是三丁基锡与二丁基锡 )。通过考察该方法标准曲线、检出限和回收率 ,结果表明其灵敏度高、定量准确、重现性好。适合于测定纺织品中的可溶出有机锡。
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| 关 键 词： | 气相色谱-质谱 有机锡 三丁基锡(TBT) 二丁基二锡(DBT) 纺织品 |
| 文章编号： | 1004-2997(2005)01-59-03 |
| 收稿时间： | 2004-06-21 |
| 修稿时间： | 2004-06-21 |
Determination of the Organotin in Textiles by Gas Chromatography-Mass Spectrometry |
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| HU Zhi-guo. Determination of the Organotin in Textiles by Gas Chromatography-Mass Spectrometry[J]. Journal of Chinese Mass Spectrometry Society, 2005, 26(1): 59-59 |
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| Authors: | HU Zhi-guo |
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| Abstract: | A extraction with acidic sweat, gas chromatography-mass spectrometry(GC/MS) method was developed to assay the soluble organotin compounds (tributyltin and dibutyltin) in the textiles. The standard curve, detection limits and recoveries were investigated, respectively. The results showed that the method is sensitive, accurate and suitable for the analysis of the soluble organotin compounds in the textiles. |
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| Keywords: | gas chromatography-mass spectrometry organotin dibutyltin tributyltin textile |
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