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Effect of water of crystallization on synthesis of nanocrystalline ceria by non-hydrolytic method
Authors:M Kamruddin  PK Ajikumar  R Nithya  G Mangamma  AK Tyagi  Baldev Raj
Affiliation:Metallurgy and Materials Group, Indira Gandhi Centre for Atomic Research, Kalpakkam, India
Abstract:Nanocrystalline ceria has been synthesized by a non-hydrolytic method using organic solvent and precipitant. The effect of the source compound on final nanocrystalline powder was investigated. The cerium nitrate hexahydrate subjected to different vacuum/thermal treatments to get cerium source compound having different extent of water of crystallization. The nanoceria, synthesized from these compounds was characterized by TGA-MS, XRD, HR-TEM and AFM.
Keywords:Nanocrystalline materials  Ceria  Non-hydrolytic synthesis  AFM  TGA-MS
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