| 2-甲基磺酰-4,6-二甲氧基嘧啶的合成及应用 |
| |
| 引用本文： | 范钱君,沈德隆,陈建强. 2-甲基磺酰-4,6-二甲氧基嘧啶的合成及应用[J]. 精细化工中间体, 2005, 35(2): 39-41 |
| |
| 作者姓名： | 范钱君 沈德隆 陈建强 |
| |
| 作者单位： | 浙江工业大学,农药研究所,浙江,杭州,310014;浙江省化工研究院,浙江,杭州,310012 |
| |
| 摘 要： | 以硫脲和丙二酸二乙酯为初始原料合成2甲基磺酰4,6二甲氧基嘧啶,总收率为62.3%(以硫脲为基准),其合成路线新颖、简便。2甲基磺酰4,6二甲氧基嘧啶是农药合成的重要中间体,特别在绿色农药新品种2嘧啶氧基N芳基苄胺衍生物的合成中。
|
| 关 键 词： | 2-甲基磺酰-4 6-二甲氧基嘧啶 合成 2-嘧啶氧基-N-芳基苄胺衍生物 应用 |
| 文章编号： | 1009-9212(2005)02-0039-03 |
| 修稿时间： | 2004-10-08 |
Synthesis and Application Reasearch of 4,6-Dimethoxy-2-methylsulfonylpyrimidine |
| |
| FAN Qian-jun,SHEN De-long,CHEN Jian-qiang. Synthesis and Application Reasearch of 4,6-Dimethoxy-2-methylsulfonylpyrimidine[J]. Fine Chemical Intermediates, 2005, 35(2): 39-41 |
| |
| Authors: | FAN Qian-jun SHEN De-long CHEN Jian-qiang |
| |
| Affiliation: | FAN Qian-jun~ |
| |
| Abstract: | Dimethoxy-2-methylsulfonylpyrimidine is an important intermediate for pesticide, especially for the preparation of 2-(2′-pyrimidyloxy)-N-het/aryl-benzylamine derivatives, a class of green novel herbicide. It was synthesized using sulphur urea and diethyl malonate as raw materials with yield of 62.3%. The process is simple and viable. |
| |
| Keywords: | 4,6-Dimethoxy-2-methylsulfonylpyrimidine 2-(2′-pyrimidyloxy)-N-het/aryl-benzylamine derivatives synthesis application |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
