| 溶剂热技术制备Ni3S2纳米粉体 |
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| 引用本文： | 郭传华,单楠楠,刘美英. 溶剂热技术制备Ni3S2纳米粉体[J]. 辽宁化工, 2010, 39(1): 1-3 |
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| 作者姓名： | 郭传华 单楠楠 刘美英 |
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| 作者单位： | 辽宁师范大学化学化工学院,功能材料化学研究所,辽宁,大连,116029 |
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| 基金项目： | 国家自然科学基金(20803033);;教育部留学回国人员科研启动基金项目资助 |
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| 摘 要： | 以硝酸镍和硫脲作镍源及硫源，以乙二醇作溶剂，采用溶剂热技术成功地制备了Ni3S2纳米粉体。用X射线粉末衍射（XRD）和透射电镜（TEM）对Ni3S2粉体的结构及形貌进行表征，结果表明反应温度和物料配比是影响Ni3S2粉体的结构和形貌的重要因素。
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| 关 键 词： | 溶剂热合成 乙二醇 Ni3S2 |
Preparation of Ni3S2 Nanoparticles by Solvothermal Method |
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| GUO Chuan-hua,SHAN Nan-nan,LIU Mei-ying. Preparation of Ni3S2 Nanoparticles by Solvothermal Method[J]. Liaoning Chemical Industry, 2010, 39(1): 1-3 |
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| Authors: | GUO Chuan-hua SHAN Nan-nan LIU Mei-ying |
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| Affiliation: | Institute of Chemistry for Functionalized Materials/a>;College of Chemistry and Chemical Engineering/a>;Liaoning Normal University/a>;Dalian 116029/a>;China |
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| Abstract: | Ni3S2nanocrystals was synthesized from nickel nitrate and thiourea with ethylene glycol as solvent by solvothermal process.The products were characterized by XRD and TEM.The results show that both the temperature and the molar ratio of nickel nitrate to thiourea have a significant effect on the phase and morphology of nickel sulfide powders. |
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| Keywords: | Solvothermal Synthesis Ethylene Glycol Ni3S2 |
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