| 芒果皮挥发性成分提取的SPME条件优化研究 |
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| 引用本文： | 黄丽,韦保耀,滕建文,夏宁.芒果皮挥发性成分提取的SPME条件优化研究[J].食品科技,2012(7):255-259. |
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| 作者姓名： | 黄丽 韦保耀 滕建文 夏宁 |
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| 作者单位： | 广西大学轻工与食品工程学院 |
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| 基金项目： | 广西科技攻关项目(桂科攻1099055) |
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| 摘 要： | 固相微萃取法(Solid-phase micro-extraction,SPME)提取台农1号芒果皮中的挥发性物质,结合气相色谱法进行分析。通过设计单因素实验和正交实验对萃取头种类、萃取时间、温度、NaCl、解吸时间进行优化。最佳萃取条件为:100μmPDMS萃取头,温度50℃、萃取时间30min、解吸时间6min,此条件下萃取获得总挥发物含量为50344.95μg/kg,异松油烯含量36676.22μg/kg,RSD分别为8.28%和6.53%。
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| 关 键 词： | 台农1号 芒果皮 挥发性成分 固相微萃取法 |
Optimization SPME conditions of volatiles in mango peel |
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| HUANG Li,WEI Bao-yao ,TENG Jian-wen,XIA Ning.Optimization SPME conditions of volatiles in mango peel[J].Food Science and Technology,2012(7):255-259. |
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| Authors: | HUANG Li WEI Bao-yao TENG Jian-wen XIA Ning |
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| Affiliation: | (Institute of Light Industry and Food Engineering,Guangxi University,Nanning 530004) |
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| Abstract: | Volatile compounds of Tainong No.1 mango peel were extracted by solid-phase micro-extraction(SPME) and detected by gas chromatography.Through single-factor and orthogonal experimental design,the fibers,extraction time and temperature,sodium chloride concentration and desorption time were optimized.The optimal extraction conditions:coating type of 100 μm PDMS,50 ℃ water bath for 30 min,and desorption of 6 min.A total content of 50344.95 μg/kg of volatile compounds was achieved under the above conditions,as to terpinolene it was 36676.22 μg/kg.The RSD were 8.28% and 6.53% respectively. |
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| Keywords: | Tainong No 1 mango peel volatile compounds SPME |
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