| 固相微萃取-气相色谱-质谱法分析香水百合的头香成分 |
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| 引用本文： | 沈文胜,芮 昶,曹 慧,李祖光. 固相微萃取-气相色谱-质谱法分析香水百合的头香成分[J]. 质谱学报, 2006, 27(Z1): 101-102 |
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| 作者姓名： | 沈文胜 芮 昶 曹 慧 李祖光 |
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| 作者单位： | 1. 杭州市质量技术监督检测院，浙江 杭州 310004; 2. 浙江工业大学化学工程与材料学院 ，浙江 杭州 310014 |
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| 摘 要： |
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Analysis of Headspace Volatiles Emitted from Fresh Fowers of lilium. spp by Gas Chromatography-Mass Spectrometry with Solid-phase Microextraction |
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| SHEN Wen-sheng,REI Chang,CAO Hui,LI Zu-guang. Analysis of Headspace Volatiles Emitted from Fresh Fowers of lilium. spp by Gas Chromatography-Mass Spectrometry with Solid-phase Microextraction[J]. Journal of Chinese Mass Spectrometry Society, 2006, 27(Z1): 101-102 |
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| Authors: | SHEN Wen-sheng REI Chang CAO Hui LI Zu-guang |
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| Affiliation: | 1.Hangzhou Institute of Calibration and Testing for Quality and Technical Supervising, Hangzhou 310004, China；2.College of Chemical Engineering, Zhejiang University of Technology, Hangzhou 310014, China
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| Abstract: | The headspace constituents released from fresh flowers of lilium. spp were sampled by solid phase microextraction(SPME). The chemical constituents were separated and identified by gas chromatography-mass spectrometry. Linalol（59.64%）, trans-ocimene（30.35%）, benzene, 1,4-dimethoxy（2.03%）, benzoic acid, methyl ester（1.69%）, phenol, 2-methoxy-4-(1-propenyl), (E)-（1.69%）,β-pinene（1.56%） were the most abundant volatiles released from fresh flowers of lilium. spp and a total of 23 volatile compounds were identified in this study. The results demonstrated that headspace SPME-GC/MS is a simple, rapid and solvent free method suitable for analysis of volatile compounds emitted from fresh flowers of lilium. spp. |
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| Keywords: | solid-phase microextraction(SPME) gaschromatography-massspectrome try（GC/MS） lilium.spp |
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