| 2，4－二硝基二苯甲酮的优化合成 |
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| 引用本文： | 郝会雷,姜日善.2，4－二硝基二苯甲酮的优化合成[J].延边大学理工学报,2009,35(3):246-248. |
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| 作者姓名： | 郝会雷 姜日善 |
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| 作者单位： | 延边大学理学院,化学系,吉林,延吉,133002 |
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| 摘 要： | 以甲苯为原料，以正交实验优化反应条件，高收率地合成了2，4-二硝基二苯甲酮．产品结构经核磁、红外光谱、质谱和元素分析进行表征．产品纯度经HPLC／MSD测定为98．24％．
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| 关 键 词： | 甲苯 2 4二硝基二苯甲酮 正交实验 |
Optimisation Synthesis of (2,4-Dinitrophenyl)(Phenyl)Methanone |
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| HAO Hui-lei,JIANG Ri-shan.Optimisation Synthesis of (2,4-Dinitrophenyl)(Phenyl)Methanone[J].Journal of Yanbian University (Natural Science),2009,35(3):246-248. |
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| Authors: | HAO Hui-lei JIANG Ri-shan |
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| Affiliation: | ( Department of Chemistry, College of Sciences, Yanbian University, Yanji 133002, China ) |
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| Abstract: | Efficient synthesis （2,4-dinitrophenyl）（phenyl）methanone were prepared from toluene. The reaction conditions were optimized by orthogonal experiment. The structure of product was confirmed with NMR, IR spectrum, MS and Elemental analysis, the purity （98.24%） of product was confirmed with HPLC/MSD. |
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| Keywords: | toluene （2 4-dinitrophenyl） （phenyl） methanone orthogonal experiment |
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