| (2,6-二甲基苯基)肼基甲酸-β-氯乙酯高效液相色谱分析 |
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| 引用本文： | 李薇,孙铁刚,徐晖,韩红娥. (2,6-二甲基苯基)肼基甲酸-β-氯乙酯高效液相色谱分析[J]. 应用化工, 2006, 35(3): 230-231 |
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| 作者姓名： | 李薇 孙铁刚 徐晖 韩红娥 |
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| 作者单位： | 西安近代农药科技股份有限公司,陕西,西安,710065 |
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| 摘 要： | 采用高效液相色谱法,以C18柱和紫外检测器,甲醇+水(80+20)为流动相,在200 nm波长,测定(2,6-二甲基苯基)肼基甲酸-β-氯乙酯的含量,结果表明,本方法的标准偏差为0.1474,变异系数为0.1705%,平均回收率为99.8%,线性相关系数为0.9998。
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| 关 键 词： | (2,6-二甲基苯基)肼基甲酸-β-氯乙酯 高效液相色谱 分析 |
| 文章编号： | 1671-3206(2006)03-0230-02 |
| 收稿时间： | 2005-11-19 |
| 修稿时间： | 2005-11-19 |
Analytical method for hydrazinecarboxylic acid,2-(2,6-dimethylphenyl)-β-chloroethyl ester by HPLC |
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| LI Wei,SUN Tie-gang,XU Hui,HAN Hong-e. Analytical method for hydrazinecarboxylic acid,2-(2,6-dimethylphenyl)-β-chloroethyl ester by HPLC[J]. Applied chemical industry, 2006, 35(3): 230-231 |
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| Authors: | LI Wei SUN Tie-gang XU Hui HAN Hong-e |
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| Abstract: | This paper introduced a quantitative analytical method for hydrazinecarboxylic acid,2-(2,6-dimethylphenyl)-β-chloroethyl ester by reverse phase HPLC with C_(18) column and UV detector at 200 nm wavelength,using methanol and water(80∶20) as mobile phase with flow rate of 1.0 mL/min.The results showed that the standard deviation was 0.1474,the variation coefficient was 0.1705%,the average recovery was 99.8%,the liner correlation was 0.9998. |
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| Keywords: | hydrazinecarboxylic acid,2-(2,6-dimethylphenyl)β-chloroethyl ester HPLC analysis |
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