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不同射频溅射功率下直接制备Ca_2Si薄膜(英文)
引用本文:杨吟野,谢泉,王义,曾正,罗胜耘.不同射频溅射功率下直接制备Ca_2Si薄膜(英文)[J].测试技术学报,2009,23(5):402-406.
作者姓名:杨吟野  谢泉  王义  曾正  罗胜耘
作者单位:1. 贵州民族学院物理系,贵州,贵阳,550025
2. 贵州大学电子科学与信息技术学院,贵州,贵阳,550025
基金项目:National Natural Science Foundation of China,the Foundation of Science Technology Department of Guizhou Province(,the Key Foundation of Education Department of Guizhou(2006212).The specific Foundation of the High-level Talents of Guizhou Province 
摘    要:磁控溅射系统在恒定Ar气压和Ar气流流量下,使用不同射频溅射功率在Si(100)衬底上分别沉积Ca薄膜;随后,800℃真空退火1 h.立方相的Ca2Si薄膜首次、单独、直接生长在Si(100)衬底上.实验结果指出,在多相共生的Ca-Si化合物中,沉积Ca薄膜时的射频溅射功率影响了立方相Ca2Si薄膜的质量;最优化的溅射功率是85 W.另外,退火温度为800℃时,有利于单一相Ca2Si的独立生长.并且,退火时间也是关键因素.

关 键 词:射频溅射  形核  退火  半导体硅化物

Directly Grown Ca_2Si Films on Si(100) Substrate at Various Radio-Frequency Sputtering Power
YANG Yinye,XIE Quan,WANG Yi,ZENG Zheng,LUO Shengyun.Directly Grown Ca_2Si Films on Si(100) Substrate at Various Radio-Frequency Sputtering Power[J].Journal of Test and Measurement Techol,2009,23(5):402-406.
Authors:YANG Yinye  XIE Quan  WANG Yi  ZENG Zheng  LUO Shengyun
Affiliation:YANG Yinye1,XIE Quan2,WANG Yi2,ZENG Zheng1,LUO Shengyun1 (1.Dept.of Physics,Guizhou University for Ethnic Minorities,Guiyang 550025,China,2.College of Electronic Science & Information Technology,Guizhou University,China)
Abstract:Ca films were directly deposited on Si(100) substrates by Radio Frequency (R. F.) magnetron sputtering system (MS) under the different sputtering power and subsequent were annealed at 800 ℃ for lh in a vacuum furnace. The structural and morphological features of the resultant films were tested by XRD, FT-IR, SEM and EDAX. The cubic phase Ca2Si film was grown directly and individually on Si(100) substrate for the first time. The experimental result indicate that the selective growth of a single phase Ca-silicide in Ca-Si system of the existence of multiple silicide phases depends on sputtering conditions, annealing temperature and annealing time. The optimal sputtering power is 85 W for the cubic phase Ca2Si film growth. Besides, 800 ℃ is the adaptive annealing temperature for Ca2Si film growth. Additionally, annealing time is also a principal factor for CazSi film growth.
Keywords:Ca2Si  Ca2Si  R  F  MS  nucleation  annealing  semiconducting silicides
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