| 含丙烯酰基可聚合色素中间体的合成 |
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| 引用本文： | 吴致宁,庄剑.含丙烯酰基可聚合色素中间体的合成[J].精细石油化工,1992(6):26-30. |
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| 作者姓名： | 吴致宁 庄剑 |
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| 作者单位： | 大连理工大学精细化工系，大连理工大学精细化工系，大连理工大学精细化工系 |
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| 摘 要： | 采用N,N-二羟乙基苯胺(BHEA)与丙烯酸直接酯化法,合成了一类可聚合色素的重要中间体。考察了催化剂种类及用量、反应温度、物料配比等反应参数对酯化反应的影响。对酯化产物分别采用TLC和GC/MS法进行了分析和鉴定。
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| 关 键 词： | 可聚合型色素 丙烯酰基 N N-二羟乙基苯胺 丙烯酸 酯化 |
SYNTHESIS OF POLYMERIZABLE DYE INTERMEDIATES CONTAINING ACRYLOYL GROUPS |
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| Wu Zhining et al..SYNTHESIS OF POLYMERIZABLE DYE INTERMEDIATES CONTAINING ACRYLOYL GROUPS[J].Speciality Petrochemicals,1992(6):26-30. |
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| Authors: | Wu Zhining |
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| Affiliation: | Dalian University of Science & Technology |
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| Abstract: | The intermediate of Polymerizable dyes containing acryloyl groups has been synthesized by esterification of N, N-bis (2-hydroxyethyl) aniline with acrylic acid. The reaction behaviors under a variety of catalysts and conditions of time, temperature and concentrations of reactant have been investigated and optimized to gain a high yield. The esterffication products were determined by TLC and GC/MS methods. |
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| Keywords: | Polymerizable Dyes Acryloyl Groups N N-bis(2-hydroxyethyl)-aniline Acrylic Acid Esterification |
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