A high-temperature accessory for measurements of the spectral characteristics of thermoluminescence |
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Authors: | A S Vokhmintsev M G Minin D V Chaykin I A Weinstein |
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Affiliation: | 1. Research and Educational Center Nanomaterials and Nanotechnologies, Yeltsin Ural Federal University, ul. Mira 19, Yekaterinburg, 620002, Russia
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Abstract: | A high-temperature accessory for a commercial fluorescence spectrometer, which allows performing luminescent studies of solid samples in the range up to 773 K, is described. The modes of linear heating with rates of 0.1–10 K/s, temperature control with an accuracy of <0.5 K, and an arbitrary temperaturetime profile were realized. The operation of a Perkin Elmer LS55 spectrometer at high temperatures was demonstrated by the example of investigating the spectral and kinetic regularities of thermoluminescence in hexagonal boron nitride using the developed module. |
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