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MoSi_2/ZrB_2基超高温陶瓷SPS制备研究
引用本文:姜子晗,汪涛.MoSi_2/ZrB_2基超高温陶瓷SPS制备研究[J].硬质合金,2011,28(1):1-7.
作者姓名:姜子晗  汪涛
作者单位:南京航空航天大学,材料科学与技术学院,江苏,南京,211106
摘    要:ZrB2具有良好的抗氧化、抗热震和抗烧蚀性能。采用放电等离子体烧结(SPS)工艺,添加体积分数为10%~20%的MoSi2烧结助剂,选取不同的烧结参数,制备出超高温陶瓷成品。经测试,ZrB2-15%MoSi2(体积分数)体系的陶瓷致密度可达99.88%,维氏硬度可达1 612,通过SEM分析,该陶瓷具有典型的核(ZrB2)-壳(MoSi2、MoB)结构,可以作为高超声速飞行器热防护用陶瓷材料的候选方案。

关 键 词:ZrB2  放电等离子体烧结  超高温陶瓷

MoSi2/ZrB2-based ultra-high temperature ceramics prepared by spark plasma sintering
Jiang Zihan,Wang Tao.MoSi2/ZrB2-based ultra-high temperature ceramics prepared by spark plasma sintering[J].Cemented Carbide,2011,28(1):1-7.
Authors:Jiang Zihan  Wang Tao
Affiliation:Jiang Zihan Wang Tao(Nanjing university of aeronautics and astronautics,Faculty of materials science and technology,Nanjing Jiangsu 211106,China)
Abstract:ZrB2 has good performance of oxidation resistance,thermal shock resistance and ablation resistance.Using 10%~20% volume ratio of MoSi2 sintering additives and different sintering parameters,ZrB2-based ultra-high temperature ceramics were prepared by spark plasma sintering(SPS) technique.The relative density and hardness of the ZrB2-based ceramics with 15vol.% of MoSi2 are 99.88% and 1 612 respectively.SEM observations show that this ceramic has typical core(ZrB2)-shell(MoSi2 and MoB) structure.This ceramics...
Keywords:ZrB2
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